Microstructure evolution in high-pressure phase transformations of CrFeNi and CoCrFeMnNi alloys

Chun Chieh Wang*, Ji Heng Chen, Jien Wei Yeh, Su Jien Lin, Shou Yi Chang, Yu Chieh Lo, Chao Chun Yen, Kuan Hao Lin, Chieh Min Tseng, Tu Ngoc Lam, Shin An Chen, Chan Sheng Wu, Chung Kai Chang, Bi Hsuan Lin, Mau Tsu Tang, Hwo Shuenn Sheu, Shi Wei Chen, E. Wen Huang

*此作品的通信作者

研究成果: Article同行評審

摘要

The extraordinary dynamics of microstructures, such as various dislocations, stacking faults, twinning, and polymorphism transformations, dominate the mechanical performance of high-entropy alloys. To reveal the phase transformation kinetics, we precisely detect the microstructure evolution in CoCrFeMnNi high-entropy alloy (HEA) and CrFeNi medium-entropy alloy (MEA) subjected to high-pressure compression using in situ angular-dispersive synchrotron X-ray diffraction. We find that controlling the initial microstructural state using cold-rolling can significantly reduce the stacking fault energy of CoCrFeMnNi and CrFeNi alloys, which results in lower onset pressures for phase transformations. The microstructure-induced stacking-fault energy reduction facilitates the formation of twins, which can act as nucleation sites for hexagonal close-packed (HCP) phase formation and recrystallization. The microstructure evolution-driven deviatoric deformation mechanism of CoCrFeMnNi HEA and CrFeNi MEA under quasi-hydrostatic compression is explored. Beyond the FCC phase, twinning in the HCP phase of CoCrFeMnNi alloy under high pressure is observed for the first time. This implies that the deformation mechanism of CoCrFeMnNi HEAs in the HCP phase is dominated by twinning-induced plasticity, which is verified using transmission electron microscopy.

原文English
文章編號165383
期刊Journal of Alloys and Compounds
918
DOIs
出版狀態Published - 15 10月 2022

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