Immobilization of β-cyclodextrin in chitosan beads for separation of cholesterol from egg yolk

Shao Hua Chiu; Tze Wen Chung; R. Giridhar; Wen Teng Wu

doi:10.1016/j.foodres.2003.12.001

Immobilization of β-cyclodextrin in chitosan beads for separation of cholesterol from egg yolk

Shao Hua Chiu, Tze Wen Chung, R. Giridhar, Wen Teng Wu^*

^*此作品的通信作者

生物醫學工程學系

研究成果: Article › 同行評審

92 引文斯高帕斯（Scopus）

摘要

Immobilization of β-cyclodextrin to chitosan beads (Ch-BCD) by cross-linking with 1,6-hexamethylene diisocyanate (HMDI) reagent has been successfully developed and demonstrated that it possessed excellent capacity for cholesterol adsorption from egg yolk. Under optimum conditions, a maximum β-cyclodextrin (BCD) loading of 0.43 g/g-chitosan was obtained. The experimental data on cholesterol adsorption fitted well in the Langmuir isotherm equation with a maximum adsorption capacity (N_m) of cholesterol 0.33 g cholesterol/g-adsorbent. 92% of the cholesterol was removed from a 30-fold diluted yolk solution at 25°C using 1% (w/v) Ch-BCD in 2 h. On the other hand, 96% of adsorbed cholesterol could be dissociated from the Ch-BCD using 95% ethanol at 50°C. In addition, the Ch-BCD retained 84% adsorption capacity after 12 reuses.

原文	English
頁（從 - 到）	217-223
頁數	7
期刊	Food Research International
卷	37
發行號	3
DOIs	https://doi.org/10.1016/j.foodres.2003.12.001
出版狀態	Published - 4月 2004

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10.1016/j.foodres.2003.12.001

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@article{dbfe155df1e041e983c0dd58473e99db,

title = "Immobilization of β-cyclodextrin in chitosan beads for separation of cholesterol from egg yolk",

abstract = "Immobilization of β-cyclodextrin to chitosan beads (Ch-BCD) by cross-linking with 1,6-hexamethylene diisocyanate (HMDI) reagent has been successfully developed and demonstrated that it possessed excellent capacity for cholesterol adsorption from egg yolk. Under optimum conditions, a maximum β-cyclodextrin (BCD) loading of 0.43 g/g-chitosan was obtained. The experimental data on cholesterol adsorption fitted well in the Langmuir isotherm equation with a maximum adsorption capacity (Nm) of cholesterol 0.33 g cholesterol/g-adsorbent. 92% of the cholesterol was removed from a 30-fold diluted yolk solution at 25°C using 1% (w/v) Ch-BCD in 2 h. On the other hand, 96% of adsorbed cholesterol could be dissociated from the Ch-BCD using 95% ethanol at 50°C. In addition, the Ch-BCD retained 84% adsorption capacity after 12 reuses.",

keywords = "Adsorption, Chitosan, Cholesterol, Egg yolk, β-Cyclodextrin",

author = "Chiu, {Shao Hua} and Chung, {Tze Wen} and R. Giridhar and Wu, {Wen Teng}",

year = "2004",

month = apr,

doi = "10.1016/j.foodres.2003.12.001",

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pages = "217--223",

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T1 - Immobilization of β-cyclodextrin in chitosan beads for separation of cholesterol from egg yolk

AU - Chiu, Shao Hua

AU - Chung, Tze Wen

AU - Giridhar, R.

AU - Wu, Wen Teng

PY - 2004/4

Y1 - 2004/4

N2 - Immobilization of β-cyclodextrin to chitosan beads (Ch-BCD) by cross-linking with 1,6-hexamethylene diisocyanate (HMDI) reagent has been successfully developed and demonstrated that it possessed excellent capacity for cholesterol adsorption from egg yolk. Under optimum conditions, a maximum β-cyclodextrin (BCD) loading of 0.43 g/g-chitosan was obtained. The experimental data on cholesterol adsorption fitted well in the Langmuir isotherm equation with a maximum adsorption capacity (Nm) of cholesterol 0.33 g cholesterol/g-adsorbent. 92% of the cholesterol was removed from a 30-fold diluted yolk solution at 25°C using 1% (w/v) Ch-BCD in 2 h. On the other hand, 96% of adsorbed cholesterol could be dissociated from the Ch-BCD using 95% ethanol at 50°C. In addition, the Ch-BCD retained 84% adsorption capacity after 12 reuses.

AB - Immobilization of β-cyclodextrin to chitosan beads (Ch-BCD) by cross-linking with 1,6-hexamethylene diisocyanate (HMDI) reagent has been successfully developed and demonstrated that it possessed excellent capacity for cholesterol adsorption from egg yolk. Under optimum conditions, a maximum β-cyclodextrin (BCD) loading of 0.43 g/g-chitosan was obtained. The experimental data on cholesterol adsorption fitted well in the Langmuir isotherm equation with a maximum adsorption capacity (Nm) of cholesterol 0.33 g cholesterol/g-adsorbent. 92% of the cholesterol was removed from a 30-fold diluted yolk solution at 25°C using 1% (w/v) Ch-BCD in 2 h. On the other hand, 96% of adsorbed cholesterol could be dissociated from the Ch-BCD using 95% ethanol at 50°C. In addition, the Ch-BCD retained 84% adsorption capacity after 12 reuses.

KW - Adsorption

KW - Chitosan

KW - Cholesterol

KW - Egg yolk

KW - β-Cyclodextrin

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DO - 10.1016/j.foodres.2003.12.001

M3 - Article

AN - SCOPUS:1242322135

SN - 0963-9969

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SP - 217

EP - 223

JO - Food Research International

JF - Food Research International

IS - 3

ER -

Immobilization of β-cyclodextrin in chitosan beads for separation of cholesterol from egg yolk

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